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Thermoresistive Characterization of Composite Materials
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Author: Kalon Lasater, Research Assistant, University of Delaware - Center of Composite Materials

Industry/Application Area

Composite Materials

Product Used

HZ Series (Z-Foil) VHA518-11, 1 MΩ

The Challenge

To measure small changes in electrical resistance in situ during thermomechanical analysis of composite specimens, an extremely stable and accurate reference resistor was required.

Tests were conducted over many hours under varying laboratory conditions where ceramic resistor technology introduced unwanted noise and instability.

The solution

A hermetically sealed resistor with essentially zero TCR was chosen to replace a ceramic resistor following the recommendation of Vishay Foil Resistors engineers. The new reference resistor significantly improved the stability and repeatability of the electrical resistance measurements.

The User Explains

The materials investigated were composites of carbon nanotubes and vinyl ester resin for in situ sensing and structural health monitoring applications, for example, aerospace and naval structures. Because this material changes electrical resistance under applied loads, when it is used in the matrix phase of fiber reinforced composites, the progression of stresses and damage can be measured. In practice, these applications experience large temperature gradients; therefore, characterizing how the electrical resistance of the material changes with temperature is of practical importance.

Fig. 1: Image of a specimen mounted on a thermomechanical analyzer stage.


Measurements

To make electrical resistance measurements in situ during thermomechanical analysis, a specimen was designed to meet the requirements of the thermomechanical analyzer (Fig 1.) and data acquisition device (NI-6218, National Instruments). As shown in Figure 2, the NI-6218 applied a voltage and measured the voltage drop across the reference resistor and specimen wired in series. The resistance of the specimen was determined through Ohm’s Law. Because the HZ Series resistor is extremely stable over long periods and has very low noise, it was ideal for this type of measurement. Figure 3 shows the typical results for a 0.10 wt% CNT/VE specimen. This material had a negative, but ultra-low, TCR which could be desirable in real-world applications.


Fig. 2: Electrical circuit diagram and interface with the NI-6218.

Fig. 3: Electrical resistance curve of 0.10 wt% CNT/VE specimen with ultra-low TCR.

The project was supervised by:

Erik T. Thostenson
Assistant Professor
Department of Mechanical Engineering
University of Delaware
USA, Newark, Delaware
Email: Thosten@udel.edu
Phone: (302) 831-8789
Website: sites.udel.edu/thostenson


Contact Information
  • Kalon Lasater
  • Research Assistant
  • University of Delaware - Center of Composite Materials
  • USA, Delaware,Newark
  • Email: Lasater@udel.edu
  • Phone: (302) 831-6484
Customer Statement
"I was fortunate to have a senior sales director and applications engineer visit me in my laboratory and discuss my instrument set-up and difficulties using other resistor technologies. After our meeting and a demonstration, there was no doubt that my experiments could benefit from VFR technology. The field engineer promptly followed up with my future requests and helped get my experiments completed. I think it is obvious how precision measurements of this type can benefit from Vishay Foil Resistors technology."
- Kalon Lasater
University of Delaware - Center of Composite Materials
Case Study
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